Paper The following article is Open access

The Effect of Aging and Crystallization Time on the Synthesis and Characteristics of Zeolite-Y from Malang-Quartzite Silica

, , and

Published under licence by IOP Publishing Ltd
, , Citation Sukrawati Arni et al 2020 IOP Conf. Ser.: Mater. Sci. Eng. 833 012060 DOI 10.1088/1757-899X/833/1/012060

1757-899X/833/1/012060

Abstract

The purpose of this study is to determine the effect of aging and crystallization time on the synthesis and characteristics of zeolite-Y. The raw material of silica used was obtained from the silica extraction of Malang quartzite by leaching and sol-gel methods. The extracted silica was analyzed using XRF and XRD. Synthesis of zeolite-Y was carried out using hydrothermal method by mixing NaOH, Al(OH)3, SiO2, and H2O according to the molar ratio of the elements in zeolite-Y. The aging process was carried out with time variations of 12, 24, 48 hours and the crystallization process were carried out with time variations of 6, 9, 12 hours at a 150 °C. The synthesized zeolite-Y was analyzed using XRF, XRD, FTIR, and SEM. The results showed that quartzite silica could be extracted by leaching and sol-gel methods with a yield of 99.1 wt%. The optimum condition of synthesis zeolite-Y was obtained at the aging time of 12 hours and the crystallization time of 12 hours.

Export citation and abstract BibTeX RIS

Content from this work may be used under the terms of the Creative Commons Attribution 3.0 licence. Any further distribution of this work must maintain attribution to the author(s) and the title of the work, journal citation and DOI.

Please wait… references are loading.
10.1088/1757-899X/833/1/012060