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Effect of exfoliation method on graphite oxide. A comparison between exfoliation by ball milling and sonication in different media

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Published under licence by IOP Publishing Ltd
, , Citation F M Casallas-Caicedo et al 2019 J. Phys.: Conf. Ser. 1386 012016 DOI 10.1088/1742-6596/1386/1/012016

1742-6596/1386/1/012016

Abstract

Graphene oxide and reduced graphene have been exfoliated from graphite oxide synthesized by Hummer's method. In order to establish a comparison, the exfoliation process was performed using two different methods, high energy ball milling and sonication. Each one was studied in two different media, organic solvent N-methyl 2 pyrrolidone and deionized water, obtaining four different products. The quality of the graphene and graphene oxides was studied using Raman spectroscopy. Structural characterization was performed using X-ray diffraction technique. The presence of oxygen-containing functional groups was determined by Fourier transform infrared spectra, while the morphology was investigated by scanning electron microscopy and energy-dispersive spectroscopy. The aim of this work is present a process to obtain graphene and graphene oxide of high quality at lower cost and better environmental conditions.

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10.1088/1742-6596/1386/1/012016