We propose an implementation of the straight-line fit algorithm to evaluate data obtained as part of measurements of line structures, e.g. a grating line, which allows us to determine, at a conventional threshold value, the coordinates of the edges, the position and the width of its photometric profile as well as the related standard uncertainty contribution. These are derived for the (1 − α)100% confidence intervals with α [0, 1]. The implementation is demonstrated using data obtained by the PTB Nanometer Comparator (Fluegge and Köning 2001 Proc. SPIE 4401 275–83). The investigation revealed that large parts of the uncertainty of the position and the width of the line are due to the choice of the fit interval and the uncertainty of the determination of the minimum and maximum level of the ...

The Physikalisch-Technische Bundesanstalt (PTB) has substantially improved the quality of its local time scale UTC(PTB), which is the national realization of the international time reference Coordinated Universal Time (UTC). It serves as the basis for PTB's time services, for local clock comparisons and for international time comparisons. Since February 2010 UTC(PTB) has been realized using an active hydrogen maser (AHM) steered in frequency via a phase micro-stepper according to an algorithm which combines the frequency comparison data between the AHM and primary and commercial caesium clocks of PTB. Thereby the long-term stability and accuracy of PTB's primary clocks, in particular its fountain clock CSF1, were combined with the short-term frequency stability of the AHM. CSF1 data were used to calculate the steering on all but six days during 15 months. During the time between July 2010 and July 2011, the time difference between UTC(PTB) and UTC was always less than 6 ns and th...

The future mise en pratique for the realization of the kelvin will be founded on the melting temperatures of particular metal–carbon eutectic alloys as thermodynamic temperature references. However, at the moment there is no consensus on what should be taken as the melting temperature. An ideal melting or freezing curve should be a completely flat plateau at a specific temperature. Any departure from the ideal is due to shortcomings in the realization and should be accommodated within the uncertainty budget. However, for the proposed alloy-based fixed points, melting takes place over typically some hundreds of millikelvins. Including the entire melting range within the uncertainties would lead to an unnecessarily pessimistic view of the utility of these as reference standards. Therefore, detailed analysis of the shape of the melting curve is needed to give a value associated with some identifiable aspect of the phase transition. A range of approaches are or could be used; ...

There is a high international priority attached to activities which reduce NO _x in the atmosphere. The current level of permitted emissions is typically between 50 µmol/mol and 100 µmol/mol, but lower values are expected in the future. Currently, ambient air quality monitoring regulations also require the measurement of NO _x mole fractions as low as 0.2 µmol/mol. The production of accurate standards at these levels of mole fractions requires either dilution of a stable higher concentration gas standard or production by a dynamic technique, for example one based on permeation tubes.

The CCQM-K74 key comparison was designed to evaluate the level of comparability of National Metrology Institutes' measurement capabilities and standards for nitrogen dioxide (NO ₂) at a nominal mole fraction of 10 µmol/mol.

The measurements of this key comparison took place from June 2009 to May 2010.

Seventeen laboratories took part in this comparison...