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Spatially resolved XRF, XAFS, XRD, STXM and IR investigation of a natural U-rich clay

M A Denecke1,4, P Michel1, T Schäfer1, F Huber1, K Rickers2, J Rothe1, K Dardenne1, B Brendebach1, T Vitova1 and M Elie3

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Combined spatially resolved hard X-ray μ-XRF and μ-XAFS studies using an X-ray beam with micrometer dimensions at the INE-Beamline for actinide research at ANKA and Beamline L at HASYLAB with those from scanning transmission soft X-ray microscopy (STXM) and synchrotron-based Fourier transform infrared microspectroscopy (μ-FTIR) recorded with beam spots in the nanometer range are used to study a U-rich clay originating from Autunian shales in the Permian Lodève Basin (France). This argillaceous formation is a natural U deposit associated with organic matter (bitumen). Results allow us to differentiate between possible mechanisms leading to U enrichment: likely U immobilization via reaction with organic material associated with clay mineral. Such investigations support development of reliable assessment of the long term radiological safety for proposed nuclear waste disposal sites.


PACS

78.70.Dm X-ray absorption spectra

82.80.Ej X-ray, Mössbauer, and other gamma-ray spectroscopic analysis methods

28.41.Kw Radioactive wastes, waste disposal

78.30.Jw Organic compounds, polymers

Subjects

Soft matter, liquids and polymers

Condensed matter: electrical, magnetic and optical

Nuclear physics

Chemical physics and physical chemistry

Dates

Issue 1 (2009)



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