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A metal mixture lowers the reaction temperature of copper chloride as shown using in situ quick XAFS

Takashi Fujimori, Masaki Takaoka, Yuta Tanino, Kazuyuki Oshita and Shinsuke Morisawa

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Trace chlorinated organic compounds are generated via thermal processes. Their formation is promoted by copper chloride in solid phase such as fly ash, especially in the post-combustion zone in municipal solid waste incineration. Previously, we reported the chemical state and change of copper chloride in a single model using the in situ quick scan x-ray absorption fine structure (QXAFS). However, a real solid phase, which is a complex system involving many elements, was not simulated. In this paper, we measured the Cu-K XAFS of a metal-mixture model upon heating to discuss the effect of mixing. The in situ QXAFS technique revealed that the reaction temperature of copper was lower, compared with the single model, when a mixture was measured. The result shows that the formation mechanism of chlorinated organic compounds derived from anthropogenic thermal sources can be described more correctly.


PACS

78.70.Dm X-ray absorption spectra

89.60.-k Environmental studies

82.33.Vx Reactions in flames, combustion, and explosions

64.75.-g Phase equilibria

Subjects

Soft matter, liquids and polymers

Condensed matter: electrical, magnetic and optical

Environmental and Earth science

Chemical physics and physical chemistry

Dates

Issue 1 (2009)



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