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EXAFS study of filled skutterudites RT4Sb12(R:La,Ce,Pr,Nd,Sm, T:Fe,Ru,Os)

Kiyofumi Nitta1, Yusuke Omori2, Takafumi Miyanaga2, Katsuhiko Takegahara2, Hitoshi Sugawara3, Daisuke Kikuchi4 and Hideyuki Sato4

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The filled skutterudites RT4X12 (R: rare-earth, T: transition metal, X: pnictogen) show a variety of intriguing features by changing the combination of R, T, and X. Among them, some compounds shows characteristic feature called "rattling" that is considered as anharmonic oscillation or off-centered motion of rare-earth ions accommodated in the icosahedron cages made from pnictogen and "rattling" is suggested to contribute to the various features of this system. We applied extended X-ray absorption fine structure (EXAFS) on this system to clarify the microscopic mechanism of "rattling" motion [1]. Temperature dependence of EXAFS thermal (Debye-Waller) factors of R-Sb and T-Sb atomic pairs were analyzed by Einstein model. Thermal oscillation and static distortion are analyzed independently. From this study, we could know systematic information about "rattling" as a large amplitude oscillation of rare-earth ions and static distortion that has two types of cage space dependence.


PACS

61.05.cj X-ray absorption spectroscopy: EXAFS, NEXAFS, XANES, etc.

63.20.-e Phonons in crystal lattices

Subjects

Condensed matter: structural, mechanical & thermal

Dates

Issue 1 (2009)



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    Kiyofumi Nitta et al 2009 J. Phys.: Conf. Ser. 190 012098

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