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N – K edge NEXAFS study of the defects induced by indium implantation in GaN

M Katsikini1, F Pinakidou1, E C Paloura1, E Wendler2, W Wesch2 and R Manzke3

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N – K edge near edge X-ray absorption fine structure (NEXAFS) spectroscopy is applied in order to determine implantation-induced changes in the electronic structure of GaN. The samples were implanted with 700 keV In ions and fluencies in the range 5×1013 – 1 × 1016 ions/cm2. The NEXAFS results are discussed in combination with Rutherford backscattering (RBS) characterization which assesses the implantation induced damage. The main implantation effects on the NEXAFS spectra are: (a) a fluence-dependent broadening of the NEXAFS peaks, (b) emergence of a pre-edge shoulder (RL1) that is attributed to N split-interstitials and (c) appearance of a post-edge sharp peak (RL2) that is attributed to molecular N2 trapped in the GaN matrix. The RL2 is characterized by fine structure due to vibronic transitions that result from a change of the vibrational quantum number along with the electronic transition. The concentration of the interstitials and the N2 molecules as well as the width of the NEXAFS peaks, have a sigmoidal dependence on the logarithm of the ion fluence, following the behaviour of the defect concentration deduced from the RBS measurements.


PACS

61.72.uj III–V and II–VI semiconductors

71.20.Nr Semiconductor compounds

78.70.Dm X-ray absorption spectra

61.72.J- Point defects and defect clusters

Subjects

Condensed matter: electrical, magnetic and optical

Semiconductors

Condensed matter: structural, mechanical & thermal

Dates

Issue 1 (2009)



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