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Novel XAFS capabilities at ELETTRA synchrotron light source

Andrea Di Cicco1,2,3, Giuliana Aquilanti2, Marco Minicucci1, Emiliano Principi1, Nicola Novello2, Andrea Cognigni2 and Luca Olivi2

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The optical layout of the XAFS beamline at ELETTRA is presented along with its powerful capabilities for collecting XAFS spectra in a wide energy range 2.4 – 27 keV. Recent developments around the ensemble of available instruments made available different collection modes using various sample environments. In particular combined x-ray absorption and diffraction patterns can be collected even at high temperature using a special version of the l'Aquila-Camerino furnace and a MAR image-plate detector. An automated beamline control software allows us to perform successive measurements in different conditions without attending the beamline. Examples of XAFS and diffraction measurements, as well as single-energy temperature scans are presented showing the performances of the beamline for nanocrystalline systems and liquid metals under high temperature conditions.


PACS

78.70.Dm X-ray absorption spectra

07.05.Dz Control systems

61.25.Mv Liquid metals and alloys

61.46.Hk Nanocrystals

Subjects

Soft matter, liquids and polymers

Condensed matter: electrical, magnetic and optical

Instrumentation and measurement

Nanoscale science and low-D systems

Dates

Issue 1 (2009)



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