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XAS at the materials science X-ray beamline BL8 at the DELTA storage ring

R Frahm1, R Wagner1, A Herdt2 and D Lützenkirchen-Hecht1

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The hard X-ray beamline BL 8 at the 1.5 GeV electron storage ring DELTA is described, and experimental data of different fields of research are presented. Making use of the intense X-ray beam emitted by a superconducting wiggler, the beamline is dedicated to X-ray absorption experiments. Three different monochromator crystal pairs are permanently available for experiments in the spectral range from about 1 keV to ca. 25 keV photon energy. Results of reference materials show that high quality EXAFS data can be obtained using Si(111) and Si(311) monochromators. First measurements in the energy range between 1.2 and 5 keV have been accomplished using YB66(400) monochromator crystals. The experimental hutch accommodates a unique 6-axis diffractometer which is well suited for all kinds of diffraction and absorption experiments, including the grazing incidence geometry. The diffractometer can carry heavy loads related to non-ambient sample environments such as e.g. ultrahigh vacuum sample stages or cryostats. Here we present typical results obtained at BL8 in different areas of materials science including investigations of dilute alloys by fluorescence mode EXAFS and the study of the structural changes associated with temperature induced spin transitions of metallo-supramolecular polyelectrolyte-amphiphile-complexes.


PACS

29.20.db Storage rings and colliders

07.85.Nc X-ray and gamma-ray spectrometers

29.30.Kv X- and gamma-ray spectroscopy

41.75.Fr Electron and positron beams

78.70.Dm X-ray absorption spectra

29.27.Ac Beam injection and extraction

Subjects

Accelerators, beams and electromagnetism

Condensed matter: electrical, magnetic and optical

Nuclear physics

Instrumentation and measurement

Particle physics and field theory

Dates

Issue 1 (2009)



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