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Semi-crystalline poly(4-methyl-1-pentene) polymers for replication of high aspect ratio diffractive features

Valtteri Kalima1, Samuli Siitonen2, Petri Karvinen2, Mika Suvanto1, Markku Kuittinen2 and Tuula T Pakkanen1

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Two transparent semi-crystalline poly(4-methyl-1-pentene) copolymers (P4MP1) of different molar mass distributions were used for injection molding of high aspect ratio (height/width) diffractive gratings. High quality sub-micron and micron features with aspect ratios of 1.6:1 were obtained with low mold temperatures. According to SEM and AFM measurements, replication of the features depended on substrate thickness and polymer. The copolymer with lower Mn and Mw penetrated deeper into the feature cavities in thin substrates, but showed poorer thermal stability and replication fidelity.


PACS

61.41.+e Polymers, elastomers, and plastics

68.37.Hk Scanning electron microscopy (SEM) (including EBIC)

82.35.Jk Copolymers, phase transitions, structure

81.20.Hy Forming; molding, extrusion etc.

81.70.Pg Thermal analysis, differential thermal analysis (DTA), differential thermogravimetric analysis

68.37.Ps Atomic force microscopy (AFM)

Subjects

Soft matter, liquids and polymers

Surfaces, interfaces and thin films

Condensed matter: structural, mechanical & thermal

Chemical physics and physical chemistry

Dates

Issue 2 (February 2008)

Received 5 November 2007

Published 9 January 2008



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