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Micro-Raman thermometry for measuring the temperature distribution inside the microchannel of a polymerase chain reaction chip

Soo Ho Kim1, Jermim Noh1, Min Ku Jeon1, Ki Woong Kim1, Luke P Lee2 and Seong Ihl Woo1

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The temperature distribution inside the microchannel was first measured using a micro-Raman spectroscopy system. Polymerase chain reaction (PCR) inside the microchannel, which is very sensitive to temperature change, was chosen to validate a novel thermometry. The micro PCR chip was fabricated by silicon micromachining. The microchip consisted of a microchannel inside the chip, a Pt film heater and a Pt film sensor on the silicon surface. The O–H stretch vibration mode of water was analyzed using a micro-Raman spectroscopy system. Its spectral changes were calibrated with temperature. The intensity ratio of the hydrogen-bonded (HB) to non-hydrogen-bonded (NHB) O–H stretch vibration modes has a linear relation with temperature. The temperature of the microchannel controlled at 55 °C varied from 53.6 to 54.8 °C depending on the location of the microchannel.


PACS

85.85.+j Micro- and nano-electromechanical systems (MEMS/NEMS) and devices

Subjects

Electronics and devices

Nanoscale science and low-D systems

Dates

Issue 3 (March 2006)

Received 1 August 2005, in final form 6 January 2006

Published 6 February 2006



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