Real-time transmission electron microscope observation of gold nanoclusters diffusing into silicon at room temperature

Author

Tadashi Ishida 1, Yuuki Nakajima 1, Junji Endo 2, Dominique Collard 3 and Hiroyuki Fujita 1

Affiliations

1 University of Tokyo, Institute of Industrial Science, 4-6-1 Komaba Meguro, Tokyo 153-8505, Japan
2 FK Optical laboratory, 1-13-4 Nakano Niiza Saitama, 352-0005, Japan
3 LIMMS/CNRS-IIS (UMI 2820), Institute of Industrial Science, The University of Tokyo, 4-6-1 Komaba, Meguro-ku, Tokyo 153-8505, Japan

E-mail

tadashii@iis.u-tokyo.ac.jp

Journal

Nanotechnology Create an alert RSS this journal

Issue

Volume 20, Number 6

Citation

Tadashi Ishida et al 2009 Nanotechnology 20 065705

doi: 10.1088/0957-4484/20/6/065705


 
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Abstract

Gold diffusion into silicon at room temperature was observed in real time with atomic resolution. Gold nanoclusters were formed on a silicon surface by an electrical discharge between a silicon tip and a gold coated tip inside an ultrahigh-vacuum transmission electron microscope (TEM) specimen chamber. At the moment of the gold nanocluster deposition, the gold nanoclusters had a crystalline structure. The crystalline structure gradually disappeared due to the interdiffusion between silicon and gold as observed after the deposition of gold nanoclusters. The shape of the nanocluster gradually changed due to the gold diffusion into the damaged silicon. The diffusion front between silicon and gold moved toward the silicon side. From the observations of the diffusion front, the gold diffusivity at room temperature was extracted. The extracted activation energy, 0.21 eV, matched the activation energy in bulk diffusion between damaged silicon and gold. This information is useful for optimizing the hybridization between solid-state and biological nanodevices in which gold is used as an adhesive layer between the two devices.

 
PACS

68.37.Lp Transmission electron microscopy (TEM)

85.85.+j Micro- and nano-electromechanical systems (MEMS/NEMS) and devices

61.46.Bc Structure of clusters (e.g., metcars; not fragments of crystals; free or loosely aggregated or loosely attached to a substrate)

68.35.Fx Diffusion; interface formation

87.85.Qr Nanotechnologies-design

Subjects

Electronics and devices

Surfaces, interfaces and thin films

Nanoscale science and low-D systems

Dates

Issue 6 ( 11 February 2009)

Received 19 September 2008 , in final form 13 November 2008

Published 15 January 2009



  1. Real-time transmission electron microscope observation of gold nanoclusters diffusing into silicon at room temperature

    Tadashi Ishida et al 2009 Nanotechnology 20 065705

  2. New quadrupole and forbidden lines in the L emission spectrum of cerium 58

    B G Gokhale and S N Shukla 1970 J. Phys. B: At. Mol. Phys. 3 1392

  3. A disintegrating cosmic string

    J B Griffiths and P Docherty 2002 Class. Quantum Grav. 19 L109

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