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Quantitative mechanical characterization of materials at the nanoscale through direct measurement of time-resolved tip–sample interaction forces

M Balantekin, A G Onaran and F L Degertekin

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We introduce a new method for material characterization at the nanoscale using a recently developed atomic force microscope (AFM) probe. The FIRAT (force sensing integrated readout and active tip) probe is integrated into a commercial AFM system to obtain time-resolved interaction forces (TRIFs) between the probe tip and sample at speeds suitable for nondestructive and fast imaging of material properties. We present a basic interaction model to extract the material elasticity and surface energy. Numerical simulations are performed and compared to the experimental results for three different polymers and a silicon sample. We find that our interaction model does not completely explain the observed long-range surface forces, but it agrees fairly well with the measurements during the tip–sample contact.


PACS

68.37.Ps Atomic force microscopy (AFM)

62.25.-g Mechanical properties of nanoscale systems

62.20.D- Elasticity

81.40.Jj Elasticity and anelasticity, stress-strain relations

Subjects

Surfaces, interfaces and thin films

Condensed matter: structural, mechanical & thermal

Nanoscale science and low-D systems

Dates

Issue 8 (27 February 2008)

Received 8 October 2007, in final form 24 December 2007

Published 4 February 2008



  1. Quantitative mechanical characterization of materials at the nanoscale through direct measurement of time-resolved tip–sample interaction forces

    M Balantekin et al 2008 Nanotechnology 19 085704

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