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Real-time in situ Raman imaging of carbon nanotube growth

K Kaminska, J Lefebvre, D G Austing and P Finnie

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In the quest for control over carbon nanotube synthesis in situ imaging has the potential to become a primary tool. Here, we show that global Raman imaging enables the observation of individual nanotubes and ensembles in real time, during growth. Individual nanotubes are detected even at 875 °C. Imaging and spectroscopy measurements of nanotube growth show distinct nucleation and growth phases. The first optical images of individual nanotubes captured during growth are presented.


PACS

78.30.Na Fullerenes and related materials

64.60.Q- Nucleation

81.07.De Nanotubes

61.46.Fg Nanotubes

78.67.Ch Nanotubes

Subjects

Condensed matter: electrical, magnetic and optical

Nanoscale science and low-D systems

Condensed matter: structural, mechanical & thermal

Dates

Issue 16 (25 April 2007)

Received 19 December 2006, in final form 7 February 2007

Published 23 March 2007



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