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Measurement Science and Technology


On-line determination of thermophysical properties in an absorption calorimeter

F O Otieno, B O Kola and F N Onyango

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A Microsoft FORTRAN 77 algorithm for calculation of the thermal absorptance and emittance of materials for solar photothermal applications is presented. It replaces the Mathematica software package used for an earlier paper and uses data from sample heating and cooling histories obtained in an absorption calorimeter. The calorimeter is automated with a Z80 microprocessor system, which has an operating system (OS) and control programs resident in a block of type 2716 EPROMs with a working memory comprising Hitachi type 6116 static RAMs. The system acquires data from the sample through thermocouples, filters, amplifiers and analogue-to-digital signal converters (ADCs) for temporary storage in the on-board RAM. The raw data are uploaded to an IBM PS/2 microcomputer for display and processing. Solutions of heat balance equations of the calorimeter are computed from the transient temperature history data using analytical and numerical methods. Results obtained for commercial copper and aluminium samples using a 60 W tungsten - halogen lamp are discussed. They compare well with those from the Mathematica package.


PACS

84.30.Sk Pulse and digital circuits

07.05.Hd Data acquisition: hardware and software

07.20.Fw Calorimeters

Subjects

Electronics and devices

Instrumentation and measurement

Dates

Issue 3 (March 1997)

Received 7 August 1996, accepted for publication 20 November 1996, in final form 5 November 1996

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