Peter J Cumpson et al 2004 Meas. Sci. Technol. 15 1337 doi:10.1088/0957-0233/15/7/016
Peter J Cumpson1, Charles A Clifford1 and John Hedley2
Show affiliationsCalibration of atomic force microscope (AFM) cantilevers is necessary for the measurement of nanonewton and piconewton forces, which are critical to analytical applications of AFM in the analysis of polymer surfaces, biological structures and organic molecules. We have developed a compact and easy-to-use reference artefact for this calibration by bulk micromachining of silicon, which we call a cantilever microfabricated array of reference springs (C-MARS). Two separate reference cantilever structures, each nominally 3 µm thick, are fabricated from a single crystal silicon membrane. A binary code of surface oxide squares (easily visible in light, electron and atomic force microscopy) makes it easy to locate the position of the AFM tip along the length of the cantilevers. Uncertainty in location is the main source of error when calibrating an AFM using reference cantilevers, especially for those having spring constants greater than around 10 N m−1. This error is effectively eliminated in our new design. The C-MARS device spans the range of spring constants from 25 N m−1 down to 0.03 N m−1 important in AFM, allowing almost any contact-mode AFM cantilever to be calibrated easily and rapidly.
68.37.Ps Atomic force microscopy (AFM)
87.64.Dz Scanning tunneling and atomic force microscopy
02.70.Dh Finite-element and Galerkin methods
06.30.Bp Spatial dimensions (e.g., position, lengths, volume, angles, and displacements)
Instrumentation and measurement
Issue 7 (July 2004)
Received 31 December 2003, in final form 15 April 2004
Published 16 June 2004
Peter J Cumpson et al 2004 Meas. Sci. Technol. 15 1337
D A Korotkin 1991 Class. Quantum Grav. 8 L219
K Rajesh Nayak et al 2003 Class. Quantum Grav. 20 1217
X Song et al 2005 Phys. Med. Biol. 50 1791
E C M Young and K N Yu 1989 J. Phys. G: Nucl. Part. Phys. 15 1053
Yue Chunxiao et al 2009 J. Phys.: Conf. Ser. 188 012006
John Hunt et al 2009 J. Radiol. Prot. 29 23
S Williams et al 2008 J. Phys.: Conf. Ser. 125 012038
M V Berry et al 2005 J. Opt. A: Pure Appl. Opt. 7 685
W. M. Holmes et al 2004 Europhys. Lett. 66 464