Quick search Find article
Quick search
Find article

Double-sided laser heating system at HPCAT for in situ x-ray diffraction at high pressures and high temperatures

Y Meng, G Shen and H K Mao

Show affiliations


An overview of a YLF:Nd laser heating system at the undulator x-ray diffraction station (16ID-B) of the high-pressure collaborative access team (HPCAT) of the Advanced Photon Source is presented. Based on the double-sided laser heating technique, the system is designed with considerable effort on the mechanical and optical stabilities, features for user-friendly operation, and the capability of accommodating diamond anvil cells of various heights up to 68 mm. This system has been used for x-ray diffraction studies of a wide range of materials to over 150 GPa and above 3000 K. Applying the laser heating technique to radial x-ray diffraction studies at simultaneous high-pressure and high-temperature (PT) conditions requires heating to be conducted at variable angles relative to the x-ray direction. A rotation laser heating design is discussed.


PACS

61.05.cp X-ray diffraction

42.62.-b Laser applications

62.50.-p High-pressure effects in solids and liquids

Subjects

Optics, quantum optics and lasers

Condensed matter: structural, mechanical & thermal

Dates

Issue 25 (28 June 2006)

Received 9 February 2006, in final form 27 April 2006

Published 8 June 2006



  1. Double-sided laser heating system at HPCAT for in situ x-ray diffraction at high pressures and high temperatures

    Y Meng et al 2006 J. Phys.: Condens. Matter 18 S1097

  2. Numerical study of pressure relationships between sample and calibrant inside the diamond anvil cell

    Nathalie Conil and Abby Kavner 2006 J. Phys.: Condens. Matter 18 S1039

  3. Deviatoric stress: a nuisance or a gold mine?

    W A Bassett 2006 J. Phys.: Condens. Matter 18 S921

  4. A k-NN Method to Classify Rare Astronomical Sources: Photometric Search of Brown Dwarfs with Spitzer/IRAC

    Massimo Marengo and Mayly C. Sanchez 2009 The Astronomical Journal 138 63

  5. Advances in data reduction of high-pressure x-ray powder diffraction data from two-dimensional detectors: a case study of schafarzikite (FeSb2O4)

    B Hinrichsen et al 2006 J. Phys.: Condens. Matter 18 S1021

  6. Ultrahigh-pressure experiment with a motor-driven diamond anvil cell

    Wendy L Mao and Ho-kwang Mao 2006 J. Phys.: Condens. Matter 18 S1069

  7. Deformation textures produced in diamond anvil experiments, analysed in radial diffraction geometry

    H-R Wenk et al 2006 J. Phys.: Condens. Matter 18 S933

  8. Nonhydrostatic compression of gold powder to 60 GPa in a diamond anvil cell: estimation of compressive strength from x-ray diffraction data

    A K Singh et al 2006 J. Phys.: Condens. Matter 18 S969

  9. A Spitzer Survey of Young Stellar Clusters Within One Kiloparsec of the Sun: Cluster Core Extraction and Basic Structural Analysis

    R. A. Gutermuth et al. 2009 ApJS 184 18

  10. Effect of shear strain on the α–ε phase transition of iron: a new approach in the rotational diamond anvil cell

    Yanzhang Ma et al 2006 J. Phys.: Condens. Matter 18 S1075

Related review articles

What's this?
View review articles related to this research to gain an insight into the key trends in this subject area. Related review articles are selected based on PACS/MSC codes, and are no more than three years old.

  1. Multiparametric crystallography using the diversity of multiple scattering patterns for Bragg and diffuse waves. Method of standing diffuse waves
  2. Small-angle neutron scattering in structure research of magnetic fluids

View by subject




Export








Please login to access our web services, or create an account if you don't yet have one.

You must have cookies enabled in your web browser to be able to login.

Username
Password

Forgotten your password? Get a new one here.