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Diamond anvil cell radial x-ray diffraction program at the National Synchrotron Light Source

J Z Hu1, H K Mao2, J F Shu2, Q Z Guo1 and H Z Liu2

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During the past decade, the radial x-ray diffraction method using a diamond anvil cell (DAC) has been developed at the X17C beamline of the National Synchrotron Light Source. The detailed experimental procedure used with energy dispersive x-ray diffraction is described. The advantages and limitations of using the energy dispersive method for DAC radial diffraction studies are also discussed. The results for FeO at 135 GPa and other radial diffraction experiments performed at X17C are discussed in this report.


PACS

61.05.cp X-ray diffraction

61.66.Bi Elemental solids

62.50.-p High-pressure effects in solids and liquids

61.50.Ks Crystallographic aspects of phase transformations; pressure effects

62.20.F- Deformation and plasticity

Subjects

Condensed matter: structural, mechanical & thermal

Dates

Issue 25 (28 June 2006)

Received 21 February 2006, in final form 2 May 2006

Published 8 June 2006



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