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An integrating flame photometer for small quantities

J A Ramsay, S W H W Falloon and K E Machin

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A method is described in which the sample is dried on a platinum wire which is then thrust into an air-coalgas flame by a mechanical device. The light from the flame enters a spectrometer and the chosen lines are allowed to fall on a photo-multiplier tube. This is connected to a Miller integrator with meter presentation. The apparatus has been tested with thallium and with sodium. A deflexion of about 100 units is given by 10-3 mg of thallium and by 10-6 mg of sodium. The average error is about 3%. This method is intended for use with small volumes, e.g. 10-3 mm3 of biological fluids. The technique of measuring and manipulating these small volumes is described elsewhere.


PACS

07.60.Dq Photometers, radiometers, and colorimeters

Subjects

Instrumentation and measurement

Dates

Issue 3 (March 1951)

Received 24 August 1950



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