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Glassy states and microphase separation in cross-linked homopolymer blends

C. Wald1, A. Zippelius1 and P. M. Goldbart2

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The physical properties of blends of distinct homopolymers, cross-linked beyond the gelation point, are addressed via a Landau approach involving a pair of coupled order-parameter fields: one describing vulcanisation, the other describing local phase separation. Thermal concentration fluctuations, present at the time of cross-linking, are frozen in by cross-linking, and the structure of the resulting glassy fluctuations is analysed at the Gaussian level in various regimes, determined by the relative values of certain physical length scales. The enhancement, due to gelation, of the stability of the blend with respect to demixing is also analysed. Beyond the corresponding stability limit, gelation prevents complete demixing, replacing it by microphase separation, which occurs up to a length scale set by the rigidity of the network, as a simple variational scheme reveals.


PACS

82.70.Gg Gels and sols

61.43.-j Disordered solids

64.75.+g Solubility, segregation, and mixing; phase separation

Subjects

Soft matter, liquids and polymers

Condensed matter: structural, mechanical & thermal

Chemical physics and physical chemistry

Dates

Issue 6 (June 2005)

Received 4 November 2004, accepted for publication 18 April 2005, in final form 18 April 2005

Published 13 May 2005



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