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Absolute falling-ball viscometer: evaluation of measurement uncertainty

M Brizard1, M Megharfi1 and C Verdier2

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To reduce the uncertainties in measurements obtained by means of capillary viscometers, we developed an absolute falling-ball viscometer. The metrological characterization of this experimental bench is presented for a mineral oil with a viscosity of 30 Pa s by means of two distinct methods described in the GUM (Guide to the Expression of Uncertainty in Measurement). First, the calculation is performed using the law of propagation of uncertainties. Then, because of the increasing use of the techniques of propagation of distributions in metrology, we calculated the measurement uncertainties by a numerical Monte Carlo simulation. Both results were then compared for a confidence interval of 95%. Finally, the viscosity measurements and uncertainties obtained by the falling-ball viscometer were compared against those obtained by a capillary viscometer.


PACS

06.30.-k Measurements common to several branches of physics and astronomy

06.20.fb Standards and calibration

06.20.Dk Measurement and error theory

Subjects

Instrumentation and measurement

Dates

Issue 4 (August 2005)

Received 16 February 2005

Published 24 June 2005



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