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Effect of substrate hardness and film structure on indentation depth criteria for film hardness testing

Ilze Manika and Janis Maniks

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The indentation depth limits for the Vickers microhardness testing of amorphous, polycrystalline, multilayer and single crystal coatings were investigated. The coating/substrate hardness ratio was varied in the range from 0.01 to 20. The critical indentation depth hc, below which the substrate has a negligible effect on the hardness, was estimated from the experimentally obtained hardness versus indentation depth curves. The results show a marked effect of the coating structure on the size of the influence zone beneath the indenter. The indentation depth limits were found to increase in the row of single crystal → polycrystalline → amorphous coatings. The obtained indentation depth criteria are compared with the reference data obtained by using finite element and kinematic calculations.


PACS

68.60.Bs Mechanical and acoustical properties

62.20.Qp Friction, tribology, and hardness

68.55.-a Thin film structure and morphology

68.65.Ac Multilayers

62.25.-g Mechanical properties of nanoscale systems

81.40.Np Fatigue, corrosion fatigue, embrittlement, cracking, fracture, and failure

Subjects

Surfaces, interfaces and thin films

Nanoscale science and low-D systems

Condensed matter: structural, mechanical & thermal

Dates

Issue 7 (7 April 2008)

Received 6 August 2007, in final form 8 November 2007

Published 12 March 2008



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