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Microstructure and electrical properties of quenched AgPb18Sb1−xTe20 thermoelectric materials

T J Zhu1, F Yan, S N Zhang and X B Zhao

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Bulk AgPbmSbTe2+m compounds exhibit outstanding thermoelectric properties. It is believed that their preparation by a higher cooling rate could improve the homogeneity of these materials, and thereby one expects a certain impact on their thermoelectric properties. We have prepared AgPb18Sb1−xTe20 compounds where x = 0.0, 0.1, 0.3 and 0.5 by quenching the melts in liquid nitrogen. High-resolution transmission electron microscopy has confirmed that the homogeneity of the samples is improved with respect to the samples prepared by furnace cooling. The decrease in the electric conductivity and the increase in the absolute value of the Seebeck coefficient, we ascribe to the improved homogeneity of the samples. The same effects on the conductivity and on the Seebeck coefficient are obtained with increasing Sb content. The influence of the Sb concentration are interpreted as follows: the number of Ag–Sb pairs and thereby the widening of the energy band increase with increasing Sb content.


PACS

72.20.Pa Thermoelectric and thermomagnetic effects

72.80.-r Conductivity of specific materials

81.40.Ef Cold working, work hardening; annealing, post-deformation annealing, quenching, tempering recovery, and crystallization

68.37.Lp Transmission electron microscopy (TEM)

Subjects

Condensed matter: electrical, magnetic and optical

Semiconductors

Surfaces, interfaces and thin films

Condensed matter: structural, mechanical & thermal

Dates

Issue 11 (7 June 2007)

Received 5 March 2007, in final form 16 April 2007

Published 18 May 2007



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